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轻量化环氧树脂复合灌封材料均匀性工艺研究
作者姓名:刘智伟  王晓敏  贺云逸  顾奋彪  范传强
作者单位:中国空间技术研究院西安分院,西安 710000;西安交通大学,西安 710049
摘    要:轻量化环氧树脂灌封材料在机械、电子、航空航天等领域有着广泛的应用,轻量化环氧树脂灌封材料中不同密度的填料在固化过程中发生分层等现象,会降低环氧树脂灌封材料的均匀性并产生应力集中,影响材料的各项性能。通过向体系中加入空心玻璃微珠作为轻量化填料,并设计了偶联处理、低温凝胶工艺、添加小粒径氮化硼等不同的均匀性提升工艺方案,研究了不同工艺条件对环氧树脂灌封材料体系的密度与均匀性的影响。结果表明:偶联处理工艺对于均匀性的影响较小,无法有效抑制体系的分层现象;低温凝胶工艺与小粒径氮化硼填料的添加能够将环氧材料体系的密度差分别降低至0.069g/cm3与0.015g/cm3,显著提升了环氧树脂灌封材料的均匀性。

关 键 词:工艺研究  均匀性  密度  环氧树脂灌封料

Study on uniformity of lightweight epoxy resin composite potting material
Authors:LIU Zhiwei  WANG Xiaomin  HE Yunyi  GU Fenbiao  FAN Chuanqiang
Abstract:Lightweight epoxy resin potting materials are widely used in machinery, electronics, aerospace and other fields. The delamination of different density fillers in lightweight epoxy resin potting materials during curing will reduce the uniformity of epoxy resin potting materials and produce stress concentration, which will affect the properties of potting materials, In this paper, hollow glass beads were added to the system as lightweight fillers. Different homogeneous lifting schemes were designed, such as coupling treatment, low temperature gel technology and small particle size boron nitride. The effects of different process conditions on the density and uniformity of epoxy resin potting material system were studied. The results showed that the coupling treatment had little effect on the uniformity and could not effectively inhibit the delamination of the system; low temperature gel technology and small particle size BN filler can reduce the density difference of epoxy material system to 0.069g/cm3 and 0.015g/cm3 respectively, and significantly enhance the uniformity of epoxy resin encapsulating material.
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