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La2O3纳米晶的制备与表征
作者姓名:宇航材料工艺
作者单位::(南京理工大学化工学院 南京 210094)
摘    要:
La2O3Nanocrystals were prepared by polyethylene glycol method. The structure and morphology ofLa2O3 nanocrystals were characterized by X-ray powder diffraction(XRD), transmission electron microscope (TEM) and BET specific surface area absorptionmeter.La2O3 nanocrystals with different size of particles anddifferent type of morphology were produced at different heat-treatment temperatures. MixedLa2O3 nanocrystals of monocline and hexagonal were obtained at 600℃and completely transformed to the hexagonal phase when the heat-treatment temperatureraised above 850℃. The Raman spectra of the La2O3 nanocrystals arealso analyzed in this paper.

修稿时间:1999-02-08
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