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研究了电子束选区熔化增材制造Ti-48A1-2Cr-2Nb合金的显微组织与拉伸性能.A1含量的烧损导致显微组织呈现不均匀性,沉积态材料由较大的γ晶粒和被α2晶粒钉扎的链状细小γ晶粒组成.γ相占据89%的体积,但并未显示出明显织构;而α2相显示出14.1倍随机值的(0001)织构,其c轴与沉积方向平行.沉积态材料的室温抗拉强度达到503MPa,而塑性为0.热等静压与热处理后的材料强度稍有下降,但延伸率获得较大改善.直到800℃,双态组织TiAl-4822材料的抗拉强度仍在460MPa以上,而全片层组织材料则维持在400MPa以上. 相似文献
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对我国新研制的Nb521铌钨合金的室温及高温性能进行了研究,并对相应的微观组织进行了分析,并结合其在液体火箭发动机推力室身部的应用情况。结果表明:该铌钨合金具有优异的工艺性能及高温性能,可满足发动机对材料性能的使用要求。 相似文献
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采用电弧熔炼的方法制备了Nb-16Si-24Ti-6Cr-6Al-2Hf (原子百分数)多元铌硅系原位复合材料。进行了高温氧化试验,使用扫描电镜、能谱和X-射线衍射仪进行分析。结果表明该复合材料铸态组织主要由Nbss和β-Nb5Si3组成;经1250℃/100h静态氧化后,生成厚的氧化皮,其主要成分为CrNbO4,TiNb2O7;在氧化皮下发生严重的内氧化现象;氧优先在Nbss相中扩散并形成内氧化产物;硅化物对氧的扩散起到一定的阻挡作用;硅化物的分散分布有利于氧化皮中压应力的释放。 相似文献
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Two near single-phase NiTiNb alloys—Ni50Ti48Nb2 and Ni49.5Ti46.5Nb4—are prepared and studied by means of scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), differential scanning calorimetry (DSC) and tensile tests in order to unearth the effects of Nb-atom solid solution in NiTi phase on the yield strength induced by self-accommodation of martensite variants. The results show that the yield strength of near single-phase NiTiNb alloys varies inversely with the amount of Nb-atoms solid-dissolved in NiTi phase. From the results out of the prior and current studies, it can be surmised that the effects of Nb content on the yield strength of NiTiNb alloys in martensite state depend on the coaction. Nb solid solution weakening mechanism and β-Nb phase composite strengthening mechanism. This inference might be a satisfactory explanation to the fact that the yield strength of (NiTi)50–0.5xNbx alloys in martensite state begins with decline and then rises when the Nb content increases. 相似文献
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Phase equilibrium in Nb-Si-Mo ternary alloys (〈37.5 at.% Si) at 1 273 K and 2 073 K is investigated by using X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The partial isothermal section at 1 273 K, which contains four single-phase regions, five two-phase regions and two three-phase regions, is basically the same as that at 1 973 K. However, when the temperature increases to 2 073 K, the three-phase region of Nbss+ct-(Nb(Mo))sSi3+13-(Nb,Mo)sSi3 obviously moves towards the Nb-rich comer. This suggests that Nb-Si-Mo ternary alloys remain stable at least up to 1 973 K. 相似文献
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9Cr13Mo3Co3Nb2V马氏体不锈钢微观组织研究 总被引:2,自引:0,他引:2
对不同热处理状态下的微观组织结构进行了研究.采用物理化学相分析技术研究了9Cr13Mo3Co3Nb2V退火、淬火以及最终热处理制度下析出相的类型、含量及组成结构式.并用X射线小角散射(SAXS)(small angle x-ray scatter)分析了不同热处理制度下析出相在不同粒度间隔中的质量分布.结果表明:①9Cr13Mo3Co3Nb2V钢退火状态的组织为珠光体 碳化物(M23C6,MC和M6C),淬火状态组织为马氏体 碳化物(M23C6和MC),最终热处理状态的组织为回火马氏体 碳化物(M23 C6,MC和M3C);②小颗粒(≤300nm)碳化物析出相粒度分析表明,9Cr13Mo3Co3Nb2V钢退火、淬火状态析出相平均粒度相差不大,粗大颗粒较多,而最终热处理状态的析出相平均粒度明显减小,且细小颗粒比例较大. 相似文献
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Effect of Nb contents on microstructure and magnetic properties of FeCoNbB films has been studied. X-ray diffraction (XRD) analysis reveals that Nb plays a role in refining grain and in facilitating formation of amorphous structure. When Nb content is more than 8 at%, the films transform from crystalline to amorphous structure, accompanied by variations in magnetic properties. An unusual out-of-plane anisotropy component is consequently observed. It can be suggested that the anisotropy induced by increasing Nb contents be attributed to stress-related magnetoelastic anisotropy. The undesirable anisotropy is greatly reduced by thermal annealing, reducing film thicknesses or applying an external magnetic field together with Si addition. 相似文献