快速凝固Al－Li－Mg－Cu－Zr合金粉末除气过程中的表面反应

研究了未除气及３５０℃／２ｈ,４５０℃／２ｈ,５００℃／２ｈ除气快速凝固（ＲＳ）Ａｌ－Ｌｉ－Ｍｇ－Ｃｕ－Ｚｒ合金粉末表面结构及氧化层厚度和组成,探讨了除气过程中粉末表面的化学反应。结果表明,通常不含Ｌｉ的铝合金粉末除气工艺对ＲＳＡｌ－Ｌｉ合金的效果不明显。     

钎缝中合金粉对组织的影响

主要研究了Ｋ３合金钎缝中加入合金粉后组织的变化,尤其是硼化物的变化,并讨论了合金粉的作用和加入方式。研究结果表明,由于加入合金粉,减少了钎缝中Ｂ和Ｓｉ元素的浓度,显著减少了Ｂ和Ｓｉ的共晶相,改善了钎缝组织。显然,这是提高钎焊接头性能的有效途径。     

先驱体转化法制备改性SiC吸收剂研究

在聚碳硅烷先驱体中掺混Ｎｉ、Ｃｏ等纳米金属微粉,在Ｎ２气氛中裂解至１０００℃,得到改性碳化硅吸收剂,通过ＴＧ、ＩＲ等分析手段,研究了该裂解反应的过程,分析了裂解及热处理产物的相组成,讨论了原料中纳米金属含量、裂解（热处理）条件等地吸收剂的微波电磁参数的影响。     

CuSn预合金对金属粉末选区激光烧结过程及烧结体质量的影响

研究了CuSn预合金对Cu基金属粉末和Ni基金属粉末选区激光烧结的影响。结果表明,对于Cu-CuSn-CuP和Ni-CuSn-CuP两类合金粉末,通过合理控制激光工艺参数(特别是激光功率和扫描速率),能顺利实现粉末烧结成形,且无明显的"球化"效应和翘曲变形。对于Cu-CuSn-CuP合金,由于结构金属Cu的熔点相对较低,在一定的工艺条件下,可以通过调整CuSn的配比,得到致密的显微组织均匀的烧结件;而对于Ni-CuSn-CuP合金,结构金属Ni的熔点相对较高,虽然也可以得到较为致密的烧结件,但其微观组织存在明显的不均匀性。     

泡沫型干扰幕特种纳米粉制备技术

基于SAS过程制备特种纳米粉的基本原理,阐明了特种纳米粉晶核生成机制,提出了制备特种纳米粉的基本方法和相应的包覆技术。为满足特种纳米粉高比表面积和高纯度的性能指标制备要求,降低成本和实现大量生产提供了一种较为可行的技术方法。     

粉末高温合金FGH96的高温缺口疲劳研究

在500℃和600℃两个温度条件下,研究了第二代粉末高温合金FGH96的缺口疲劳性能,将原始数据的曲线拟合成S-N曲线,分析光滑与缺口试样的Kf的差别,用扫描电镜分析了试样的断口形貌特征。结果表明:FGH96合金的疲劳缺口敏感性随着温度的升高和应力比的增大而降低;与光滑试样的断口相比,合金的缺口试样在高温下疲劳裂纹多由加工刀痕起源,因此缩短了其疲劳萌生寿命;疲劳扩展区疲劳条带比较明显,扩展区面积比光滑试样小。     

一种高温合金粉末预处理后表面的分析

本文用ESCA及电子显微分析方法研究了预处理Rene’95粉末表面的成分及析出相情况。预处理后粉末表面出现大量ZrO_2析出。雾化粉末表面的M’C碳化物在原位转变成MC。在粉末表面上还有大量二次碳化物,这些碳化物依附表面氧化物生核长大。预处理不能减少表面析出相数量,也未改变表面析出相的类型。     

The management of stray radiation issues in space optical systems

The performance of infrared and submillimeter systems can be severely degraded by stray light. Stray light includes off-axis radiation, system diffraction and scattering effects, and thermal self-emission. The purpose of this paper is to identify several keys to preventing system degradation due to stray radiation. The first key is to apply stray light design rules and analysis techniques early in the program before the design is finalized. A systems level analysis using stray light analysis software is often necessary in order to identify more subtle problems and to assess the magnitude of their effect on system performance. Another key is to address contamination control and the choice of surface coatings early in the program. The management of stray radiation issues is extremely cost-effective, if begun early in the program, and can reduce later schedule hardships.     

Preparation and Mechanical Properties of Glass Coats with High Temperature Radar Absorber

BaO-La2O3-B2O3 (BLB) glass, suitable to be used as a sealing between metals, was chosen to be the binder in preparing glass coats on the Ti-alloy substrate. The SiCN nano-powder was introduced as the filler for the absorbing coat because it is considered to be a good high temperature absorber. The effect of the coating temperature and coating time on the tensile strength of the glass coat was investigated and the proper coating parameters to get good mechanical properties were determined. In addition, the effects of the SiCN content on the tensile strength of the absorbing coat were also discussed. Results show that it is possible to prepare the glass coat using the BLB glass as a binder. That the coat formed at 730 ℃ for 30 min has the best tensile strength witnesses 730 ℃, 30 min to be the proper parameter to prepare the glass coat. The BLB glass coat without SiCN powder possesses good tensile strength and the introduc-tion of the SiCN absorber into the glass coat will lower the tensile strength. As the SiCN content increases, the tensile strength of the absorbing coat decreases, which could be attributed to the aggregation of SiCN in the coats.     

黑火药与现代化学推进剂

本文论述了黑火药的三大组分在现代化学推进剂发展中的重要作用.黑火药是最原始的复合固体推进剂.现代化学推进剂,无论是液体推进剂或固体推进剂,都可看作是黑火药的进一步发展.并简要地介绍了复合固体推进剂的发展过程和今后的发展趋势.