共查询到19条相似文献,搜索用时 62 毫秒
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运用Ubbelohde式粘度计测定PBO/MSA和PBOT/MSA溶液的粘度,采用稀释外推法对溶液浓度和粘度的关系进行了分析。结果发现,当溶液浓度极低时,出现溶液粘度随浓度降低而增大的反常行为。通过实验研究,排除了粘度计和临界接触浓度的影响导致PBZs聚合物的极稀浓度区异常行为的可能性;同时通过加入不同浓度外加盐的方法,证明了可用半刚性聚电解质模型合理解释PBZs聚合物溶液极稀浓度区的异常行为。为了避免极稀溶液区出现反常现象,保证PBZs聚合物特性粘数测量的准确性,应尽量保证溶液的ηr=1.2~2.0。 相似文献
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HTPB聚氨酯弹性体的动态力学性能研究 总被引:2,自引:2,他引:2
用动态热机械分析法研究了固化参数,增塑剂含量,不同助剂对HTPB/TD1聚氨酯弹性体的动态力学损耗的影响。结果表明:在所研究的HTPB/TDI聚氨酯弹性体的动态力学谱中,出现了两个损耗峰:其中低温峰对应于HTPB聚合物的玻璃化转变;常温峰对应于聚合物链中硬段微区的损耗峰。 相似文献
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以2.5D针刺炭毡为增强体,酚醛树脂为先驱体,采用液相浸渍-碳化法制备C/C复合材料。对酚醛树脂先驱体溶液的流变性能、凝胶性能、固化行为及失重行为等性能进行全面的分析,为后续工艺优化提供指导,研究了酚醛树脂溶液浓度对2.5D针刺炭毡浸渍效率的影响。结果表明,当浸渍温度为60℃时,酚醛树脂溶液的粘度在4 h的浸渍时间内保持在200 m Pa·s左右,在1.5 MPa下加压浸渍3 h,循环6个周期的浸渍固化炭化工艺过程后,浓度为75%的酚醛树脂溶液的浸渍效果较好,浸渍效率高。 相似文献
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铝粉/HTPB悬浮液的流变特性 总被引:4,自引:0,他引:4
用旋转粘度计和动态流变仪研究了铝粉/HTPB悬浮液的流变特性及铝粉含量、粒度、形状对流变性的影响。结果表明:铝粉颗粒间不存在相互作用,铝粉影响流变性的主要因素是粒子形状。这一结果将有助于通过调节铝粉类型来改善推进的工艺性能。 相似文献
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《上海航天》2019,(Z1)
探索剪切力对硼粉/端羟基聚丁二烯(B/HTPB)混合体系流变性能的影响,采用旋转粘度计和同向双螺杆转矩流变仪分别考察了B/HTPB体系在低剪切应力和高剪切应力下流变特性的变化规律。结果表明:B/HTPB体系在旋转粘度计中剪切速率小于5s-1,剪切应力小于200Pa,含硼25%的B/HTPB体系在50℃下混合300min,表观粘度在26.9~32.0Pa·s内变化;而B/HTPB体系在同向双螺杆转矩流变仪中的剪切速率范围为71.11~355.56s-1,剪切应力比旋转粘度计的高1~2个数量级,对于含硼20%的B/HTPB体系在50℃、233.33s-1下混合230min,表观粘度达到446.3Pa·s,体系达到凝胶状态。在高剪切力作用下,B/HTPB体系粘度快速增加,低剪切力作用下B/HTPB体系粘度几乎不变。因此,在高剪切应力下对改性硼粉的B/HTPB体系流变规律进行研究,可为硼粉改性和团聚效果的评价提供一种方法。 相似文献
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以端羟基聚丁二烯(HTPB)为引发剂,三氟化硼乙醚络合物为催化剂,环氧丙烷为促开环剂,通过四氢呋喃的阳离子开环聚合反应,制备出聚四氢呋喃-聚丁二烯-聚四氢呋喃三嵌段共聚物(PTHF-PB-PTHF)。采用红外光谱、核磁共振氢谱及碳谱、凝胶渗透色谱-激光光散射联用技术,对目标化合物的结构进行了表征。采用相对分子质量为8 066 g/mol的PTHF-PB-PTHF与甲苯二异氰酸酯反应制备了交联弹性体,应力-应变试验显示,在相同交联密度下,PTHF-PB-PTHF交联弹性体的拉伸强度及断裂伸长率较纯HTPB交联弹性体分别提高了16%及19%。动态热机械性能分析表明,PTHF-PBPTHF交联弹性体具有优异的粘弹性能,其玻璃化转变温度为-55.99℃,低于HTPB交联弹性体。 相似文献
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Old arguments that free O(2) must have been available at Earth's surface prior to the origin of photosynthesis have been revived by a new study that shows that aerobic respiration can occur at dissolved oxygen concentrations much lower than had previously been thought, perhaps as low as 0.05?nM, which corresponds to a partial pressure for O(2) of about 4?×?10(-8) bar. We used numerical models to study whether such O(2) concentrations might have been provided by atmospheric photochemistry. Results show that disproportionation of H(2)O(2) near the surface might have yielded enough O(2) to satisfy this constraint. Alternatively, poleward transport of O(2) from the equatorial stratosphere into the polar night region, followed by downward transport in the polar vortex, may have brought O(2) directly to the surface. Thus, our calculations indicate that this "early respiration" hypothesis might be physically reasonable. 相似文献
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Both listening and transmitting may, on an existential level, be either dangerous or beneficial. So we should ignore our irrational fears and listen in the hope of detecting ETI and transmit on the basis of promoting SETI activity. 相似文献
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聚对苯撑苯并双嗯唑(PBO)纤维制备及性能研究 总被引:1,自引:0,他引:1
采用4,6-二氨基间苯二酚(DAR)与对苯二甲酸(TPA)缩聚的方法制备PBO聚合物溶液,在180—200℃使聚合物形成液晶态,利用干喷湿纺制法制备纤维。采用DSC、Raman及XRD等方法对纤维进行表征。制备的纤维与商品纤维相比,具有相同的结构和热性能,但表面形貌和强度有差异;两种纤维具有6个相同的主要Raman光谱带,但制备纤维的峰面积较小。制备的PBO纤维热降解温度达650℃,热牵伸处理可使纤维的模量提高至240~300GPa。 相似文献
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"栉"是先秦时期表示"梳头用具"义的常用词."梳"在口语中出现不晚于东汉末.在魏晋时期,"梳"和"栉"之间在文学语言中呈现同义竞争状态.南北朝时期,"梳"取代"栉"成为"梳头用具"义的常用语.隋唐时期,这种优势得到进一步强化. 相似文献
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We report the discovery of the N(2)(+) A-X Meinel band in the 780-840 nm meteor emission from two Leonid meteoroids that were ejected less than 1000 years ago by comet 55P/Tempel-Tuttle. Our analysis indicates that the N(2)(+) molecule is at least an order of magnitude less abundant than expected, possibly as a result of charge transfer reactions with meteoric metal atoms. This new band was found while searching for rovibrational transitions in the X(2)Pi electronic ground state of OH (the OH Meinel band), a potential tracer of water bound to minerals in cometary matter. The electronic A-X transition of OH has been identified in other Leonid meteors. We did not detect this OH Meinel band, which implies that the excited A state is not populated by thermal excitation but by a mechanism that directly produces OH in low vibrational levels of the excited A(2)Sigma state. Ultraviolet dissociation of atmospheric or meteoric water vapor is such a mechanism, as is the possible combustion of meteoric organics. 相似文献