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采用钴基钎料及镍基合金粉料,分别在1170℃保温10min、60min和120min的钎焊工艺下,对K452镍基铸造高温合金进行真空钎焊实验,通过扫描电镜和能谱分析仪进行了接头显微组织观察与物相分析,并测试钎焊接头的高温力学性能。结果表明:在保温60min的工艺规范下,界面实现较好的结合,钎缝内部孔洞缺陷较少,钎缝组织均匀,有利于钎焊接头性能的提高;在更长的保温时间120min下,钎缝内部又有蚀孔缺陷形成,且较多的白色块状化合物在合金粉颗粒间聚集长大,但界面结合良好,钎焊接头性能较高,900℃抗拉强度达到400MPa,900℃/100MPa持久寿命为141h55min。 相似文献
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通过GH4033合金钎焊接头界面断裂力学试验,研究了钎焊接头界面断裂行为,获得了钎焊接头界面裂纹的临界应变能释放率,分析了影响界面断裂特征的因素,为钎焊接头界面断鲜明性能评定提供了参考依据。 相似文献
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采用BNi68Cr WB粉末作为连接材料,利用真空钎焊工艺成功制备了C/C复合材料与镍基高温合金(GH600)的连接试样。并借助扫描电子显微镜和材料万能试验机,研究钎焊接头微观组织结构和室温及高温(700℃)下的抗剪切性能。结果表明,使用BNi68Cr WB粉末可以实现C/C与GH600的钎焊连接,接头的断裂位置为C/C复合材料母材;与室温条件相比,钎焊接头在700℃下的抗剪强度较低。 相似文献
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本文介绍了两种钎料的钎焊接头抗高温动态腐蚀性能,1Cr18Ni9Ti不锈钢基体表面经酸洗-镀镍或混合处理后,用一、二号合金作钎料,采用高规范钎焊的接头,其抗高温动态腐蚀性能良好。本文还对影响钎焊接头抗高温动态腐蚀性能的各种因素进行了试验。 相似文献
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采用Co50NiCrWB钎料在1160℃/15 min条件下进行了熔化润湿试验,并钎焊得到DD5与GH3039异质高温合金接头,分析了接头的显微组织和力学性能。试验结果表明,Co50NiCrWB钎料在DD5和GH3039高温合金表面的润湿性能良好,接头包括钎料反应区与扩散影响区,反应区主要物相为溶有Cr的Ni–Co基固溶体、富Cr硼化物相和富Co、Cr、W、Re的硼化物相。钎焊接头在900℃的拉伸性能平均值达到193 MPa,900℃/40 MPa下的接头持久寿命最高达到221 h。拉伸试样断口观察表明断裂发生在钎料反应区,呈脆性断裂特征。 相似文献
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采用非晶态BNi-2钎料成功实现了高铌TiAl合金与GH3536合金的连接,获得良好的钎焊接头。钎焊接头的典型界面组织为TAN/B2+τ3/τ4+(Ni-Ti)-B/γ+(Ni-Ti)-B+CrB+G相/GH3536。通过分析钎焊温度对接头界面微观组织的影响,表明BNi-2钎料中B元素的扩散以及GH3536合金向液态钎料中的溶解对界面组织结构演变起着至关重要的作用。而随着钎焊温度的升高,扩散IV区逐渐消失,接头由4个区域变为3个区域,τ3/τ4化合物层及钎缝区域均逐渐增厚,黑色CrB相发生粗化,细小点状(Ni,Ti)-B含量减少。1 160℃保温10 min时,所获得的钎焊接头最大室温及高温(700℃)抗剪强度分别为~106.8 MPa和~76.2 MPa,其剪切强度降低约28.6%,接头均呈现脆性断裂模式。接头形成过程可以划分为固相扩散、液相生成、等温扩散凝固和残余液相析出4个阶段。 相似文献
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采用Co45Ni Cr WB钴基钎料,预填FGH95镍基合金粉,在1220℃不同保温时间下对K465高温合金进行0.5 mm大间隙真空钎焊实验,研究钎缝组织构成及不同保温时间对钎缝组织与接头性能的影响。结果表明:钎缝组织由合金粉颗粒及颗粒间硼化物相构成,颗粒内为γ和γ'双相组织和少量小块状硼化相,颗粒间是高Cr,W和Nb的硼化物相;钎焊时随保温时间延长合金粉长大,化合物相合并长大;合金粉比例高、保温时间适当获得钎缝中化合物相细小弥散分布,对接头性能有利;钎焊保温30~60 min时接头持久性能较高。 相似文献
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采用Ni-Cr-B钎料分别在1120℃/10 min和1120℃/10 min/2 MPa的工艺下实现FGH96与DD6的钎焊连接。测试两种工艺下接头的抗拉强度,通过光学显微镜(OM)、扫描电子显微镜(SEM)和电子探针(EPMA)分析接头的组织、成分和断口。结果表明:真空加压钎焊所得接头的室温平均抗拉强度达到1187 MPa,远高于真空钎焊接头621 MPa的强度;与不加压的真空钎焊相比,真空加压钎焊所得FGH96/DD6接头的钎缝中心没有平行于被焊面的晶界,而是单个晶粒贯穿整个钎缝,并与母材连接面发生韧性断裂;真空钎焊接头中存在Ni3B相,而真空加压钎焊钎缝中并没有残留的Ni3B相,主要由(Ni,Cr)固溶体组成。 相似文献
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《中国航空学报》2021,34(6):67-78
The brazing of diamond is a promising way to fabricate grinding wheels for efficient machining and precision grinding. This work investigated the feasibility of bonding diamond grits onto Aluminium Alloy 7075 (AA7075) substrate with a Ag–Cu–Ti filler alloy via laser fusion brazing. The interfacial microstructures and the strength of the brazed diamond joints were studied. The cross-section of the brazed diamond joint consists of a molten filler alloy layer, a molten pool, a heat effect zone, a columnar crystal zone and an equiaxed crystal zone. Within the interface of the filler alloy/substrate metal, microstructures observed possibly were Ag(s.s), Al(s.s), TixAl, Al2Cu and Mg intermetallic compounds. A layer of TiC with a thickness of about 30–50 nm was found at the bonding interface of the diamond/filler alloy. The averaged peak shear force of the brazed joints was found to be approximately 39.8 N. The abrasion grinding test indicated that the diamond/AA7075 brazed joint was adequate for grinding. However, the pulled-off of grit was found to be the primary failure of this type of brazed joint. This work broadened the brazing diamond technique and the range of applications of brazed diamond wheels for efficient grinding. 相似文献
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吴昌忠%陈静%陈怀宁%林泉洪 《宇航材料工艺》2005,35(3):17-20,30
综述了钛及钛合金高温钎焊结构在现代工业中的应用。在分析了钛基钎料应用和发展的基础上,重点分析了钎焊接头的组织与接头性能的关系以及影响因素。指明接头组织中脆性金属间化合物相的存在形态是决定接头性能的主要因素,接头间隙和钎焊时间决定了接头的组织形态,从而影响接头的性能。钛及钛合金高温钎焊接头的拉伸性能、高温性能和疲劳性能是优越的,而接头氧化后的性能急剧下降。并展望了钛基材料连接的发展方向。 相似文献
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《中国航空学报》2020,33(1):383-390
Nano-Al2O3 particles modified AgCuNi filler was adopted to braze the SiO2 ceramic and TC4. The effects of filler size as well as the brazing temperature on the interfacial microstructure and mechanical property of the joints were investigated. Nanoscale filler reduced the phases dimension and promoted the homogeneous distribution of microstructure, obtaining a higher joint strength when compared to microscale filler. The increase of brazing temperature made the accelerating dissolution and diffusion of Ti, which promoted the increase of thickness of Ti4O7 + TiSi2 layer adjacent to SiO2 ceramic and diffusion layer zone nearby TC4 alloy. The hypoeutectic structure was produced in the brazing seam due to the high Ti content. The maximum shear strength of ∼40 MPa was obtained at 950 °C for 10 min. 相似文献
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本文利用AgCuTi-W复合钎料作中间层,在适当的工艺参数下真空钎焊Cf/SiC复合材料与Ti合金,利用SEM,EDS,XRD分析接头微观组织结构,利用剪切试验检测接头力学性能。研究结果表明:钎焊时,复合钎料中的Ti借助Cu-Ti液相与Cf/SiC复合材料反应,在Cf/SiC复合材料与连接层界面形成Ti3SiC2,Ti3Si和少量TiC化合物的混合反应层。复合钎料中的Cu与Ti合金中的Ti发生互扩散,在连接层与Ti合金界面形成不同成分的Cu—Ti化合物过渡层。钎焊后,形成W颗粒强化的致密复合连接层,W颗粒主要分布在Cu-Ti相中。W的加入缓解了接头的残余热应力,Cf/SiC/AgCuTi—W/TC4接头剪切强度明显高于CF/SiC/AgCuTi/TC4接头。 相似文献
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《中国航空学报》2021,34(4):132-139
Profiled monolayer cBN wheel was induction brazed for grinding of titanium dovetail slot in this study. Aimed at acquiring a uniform temperature distribution along the profiled surface and reducing the thermal deformation of the brazed wheel, a finite element model was established to investigate the temperature uniformity during induction brazing. A suitable induction coil and the related working parameters were designed and chosen based on the simulation results. Ag-Cu-Ti alloy and cBN grains were applied in the induction brazing experiment. The results showed geometric deformation of the brazed wheel was no more than 0.01 mm and chemical reaction layer were found on the brazed joint interface. Further validation tests were carried out by grinding of Ti-6Al-4V alloy. Compared to the electroplated wheel, the brazed wheel showed better performance such as low specific grinding energy and good ground quality in grinding of Ti-6Al-4V alloy. Abrasion wear was found to be the main failure mode for the induction brazed wheel, while adhesion and grains pull-out were the main failure mode for the electroplated wheel. 相似文献